MDA was linear from 1 to 100 μg/L, HMA from 2.5 to 100 μg/L, and MDMA, HMMA, and MDEA from 2.5 to 400 μg/L. The LOQ of each analyte was the lowest concentration on the calibration curve. MDA and HMA are found in considerably lower concentrations than MDMA and HMMA; thus, an upper limit of quantification of 100 μg/L was sufficient.

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